超声波及微波辅助萃取火麻籽油中α-亚麻酸含量的GC-MS测定.pdfVIP

56 粮食与油脂 2015 年第 28 卷第 12 期 α 超声波及微波辅助萃取火麻籽油中 - 亚麻酸 含量的GC-MS 测定 曾凡炎，马　燮，杨　郭，刘海军 （四川理工学院材料与化学工程学院，　四川自贡　643000 ） 摘　要：采用超声波以及微波辅助萃取火麻籽油，通过单因素实验确定最佳工艺条件，比较不同 α 萃取方法的油脂收率。通过气质联用仪（GC–MS ）测定油品中 – 亚麻酸的含量。实验结果表明： 超声波辅助萃取火麻籽油最佳工艺条件为料液比 1 ∶16 （g/mL ）、超声波功率180 kW、萃取时间 40 min 和萃取温度20 ℃，此时油脂最大收率为36.49%；微波辅助萃取火麻籽油最佳工艺条件为 料液比 1 ∶16 （g/mL ）、微波功率800 kW、萃取时间8 min 和萃取温度50 ℃，此时油脂最大收率为 α 37.86%；超声波与微波辅助萃取油品中 – 亚麻酸的含量分别为21.02%、26.39%。 α 关键词：火麻油；油脂收率；超声波；微波；– 亚麻酸；气相色谱– 质谱联用 Used GC-MS to analysis content of α-Linolenic acid exctrated from hemp seed oil by ultrasonic wave and microwave ZENG Fan-yan ，MA Xie ，YANG Guo ，LIU Hai-jun （College of Materials and Chemical Engineering ，Sichuan University of Science Engineering ， Zigong 643000 ，Sichuan ，China ） Abstract ：Hemp seed oil extracted by ultrasonic wave and microwave ，compared different extraction methods of oil yield ，optimum technolgical conditions were determined by single factor experiment. GC–MS was used to analysis the content of α–Linolenic acid. The results showed that a ratio of material 16 （g /mL ），ultrasonic wave power of 180 kW ，extraction time of 40 min and to solvents of 1 ∶ extraction temperature of 20 ℃ were the optimized process conditions for ultrasonic wave extraction. Under those conditions ，a maximum rate of 36.49% was obtained ；The ratio of material to solvents of 1 ∶16（g/mL ），microwave power of 800 kW ，extraction time of 8 min and extraction temperate of 50 ℃ were the optimized process conditions for microwave e